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adsorption effects, is apparent. Of particular note is the observation in Figure 17.19B, which shows that the diamond electrode retains virtually constant activity over more than 60 scans, whereas the screen carbon electrode loses more than 35 % of its activity in this period. Although electro-oxidation is the most frequently used method for the electrochemical sensing of organics, if reducible functional groups are present, the potential window of diamond in the cathodic region can again be exploited advantageously for electrochemical sensing. An example is the detection of Parathion, a harmful pesticide with a maximum permissible concentration in drinking water of around 35 g L 1 . The molecule has a reducible nitro group (NO2 ) in the structure that undergoes reduction at about 0.7 V versus SCE. As shown in Figure 17.20, this can be used to develop a sensitive analytical procedure for the detection of Parathion [24]. A limit of detection in pure water was found to be 2.9 g L 1 , well below the maximum permissible concentration, somewhat better than was achievable using a more conventional hanging mercury drop electrode (HMDE). The investigators also studied the detection of Parathion in real polluted water samples (Figure 17.20). Whilst the other pollutants have a small effect on the detection of Parathion rdlc ean 13 EAN - 13 Client Report RDLC Generator | Using free sample for EAN ...
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